色谱指纹图谱在香精香料质量控制中的应用

Application of Chromatogram Fingerprint in the Quality Control of the Flavor and Perfume

  • 摘要: 烟用香精香料化学成分复杂,现无合适的化学质量控制方法,通过实例,对10个批次正常生产的香料标样进行同时蒸馏萃取,取其萃取液进行气相色谱氢焰检测.进行同组分色谱峰的匹配,根据相对峰面积求出标准指纹图谱,然后10批标样各自与标准指纹图谱进行相似度计算,据此设立待测样品的合格性允差范围.待测样品与标准指纹图谱进行谱峰匹配,计算与标准指纹图谱的相似度,依据合格性允差范围,判定其质量状况.

     

    Abstract: The chemical composition of tobacco flavor and perfume is complicated,and there is no suitable chemical quality control method by now.In the instance taking ten batches normal samples of tobacco flavor and perfume and simultaneous distilling and extracting.After that,fetching its extracted liquid and measuring it with GC/FID.Matching the chromatogram peaks of the same kind of composition,and obtaining the standard chromatogram fingerprint according to its relatively area of each peak.Then calculating the similarity compare the ten batches of the normal samples to the standard chromatogram fingerprint,and seting up the range of the eligible sample to be measured.Matching the chromatogram peaks between the sample to be measured and the standard chromatogram fingerprint,and calculating the similarity compare the sample to be measured to the standard chromatogram fingerprint,then judging its quality state according to the range.

     

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