Abstract: In view of the problems and the present situation in the teaching of nuclear magnetic resonance (NMR), the paper introduces the reform measures for NMR in modern instrumental analysis teaching, which can contribute to the application and popularization of NMR technology. At the same time, the combination of theory and practice can stimulate students to learn the modern instrumental analysis technology and improve their practical ability and scientific research ability, and lay a foundation for the training of innovative talents of colleges and universities.